Benzene, 2-ethynyl-1,4-diMethoxy- synthesis

12synthesis methods

Product Name:Benzene, 2-ethynyl-1,4-diMethoxy-
CAS Number:22944-08-7
Molecular formula:C10H10O2
Molecular Weight:162.1852

Benzene, 1,4-dimethoxy-2-[2-(trimethylsilyl)ethynyl]-

531504-78-6
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22944-08-7
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Yield:22944-08-7 93%

Reaction Conditions:

with potassium hydroxide in methanol;chloroform;water at 20; for 0.5 h;Inert atmosphere;

References:

Yamaguchi, Yoshihiro;Matsubara, Yoshio;Ochi, Takanori;Wakamiya, Tateaki;Yoshida, Zen-Ichi [Journal of the American Chemical Society,2008,vol. 130,# 42,p. 13867 - 13869] Location in patent:supporting information; experimental part

4-METHOXYPHENYL 4-METHYLBENZENESULFONATE

3899-91-0
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22944-08-7
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References

25245-35-6
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22944-08-7
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References

98279-45-9
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22944-08-7
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References

Phenol, 3-iodo-4-methoxy-, 1-(4-methylbenzenesulfonate)

186134-37-2
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22944-08-7
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References