benzo[b]thiophen-3-yl acetate synthesis
- Product Name:benzo[b]thiophen-3-yl acetate
- CAS Number:24434-82-0
- Molecular formula:C10H8O2S
- Molecular Weight:192.23
Yield:24434-82-0 89%
Reaction Conditions:
Stage #1: N,N-diethyl-2-methylsulfanylbenzamidewith lithium diisopropyl amide in tetrahydrofuran at -78 - 20;
Stage #2: acetyl chloridewith sodium hydride in tetrahydrofuran at 20;
References:
Pradhan, Tarun Kanti;De, Asish [Tetrahedron Letters,2005,vol. 46,# 9,p. 1493 - 1495]
1696-17-9
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