Bicifadine synthesis

3synthesis methods

Product Name:Bicifadine
CAS Number:71195-57-8
Molecular formula:C12H15N
Molecular Weight:173.25

1-(p-Tolyl)-3-azabicyclo[3.1.0]hexane-2,4-dione

66504-77-6
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71195-57-8
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Yield:71195-57-8 58%

Reaction Conditions:

with sodium bis(2-methoxyethoxy)aluminium dihydride in benzene; for 2 h;Heating;

References:

Epstein, Joseph W.;Brabander, Herbert J.;Fanshawe, William J.;Hofmann, Corris M.;McKenzie, Thomas C.;et al. [Journal of Medicinal Chemistry,1981,vol. 24,# 5,p. 481 - 490]

Benzeneacetic acid, 2-bromo-4-methyl-, methyl ester

77053-52-2
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71195-57-8
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References

dimethyl 1-(4-methylphenyl)cyclopropane-1,2-dicarboxylate

66504-76-5
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71195-57-8
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References

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