BOC--BENZYL-DL-PRO-OH synthesis
- Product Name:BOC-
-BENZYL-DL-PRO-OH - CAS Number:351002-72-7
- Molecular formula:C17H23NO4
- Molecular Weight:305.37
145681-01-2
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 0.33 h / -78 - 0 °C
1.2: benzyl halide / 12 h / 20 °C
2.1: sodium hydroxide / tetrahydrofuran; methanol / 3 h / 60 °C
References:
Baumann, Marcus;Moody, Thomas S.;Smyth, Megan;Wharry, Scott [Journal of Organic Chemistry,2021,vol. 86,# 20,p. 14199 - 14206]