BOC-ASP(OBZL)-PHE-OH synthesis
- Product Name:BOC-ASP(OBZL)-PHE-OH
- CAS Number:68763-45-1
- Molecular formula:C25H30N2O7
- Molecular Weight:470.51
63-91-2
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7536-58-5
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$6.00/5g
68763-45-1
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$60.00/500mg
Yield:68763-45-1 80%
Reaction Conditions:
Stage #1: BOC-L-aspartic acid 4-benzyl esterwith 1-hydroxy-pyrrolidine-2,5-dione;dicyclohexyl-carbodiimide in tetrahydrofuran;Inert atmosphere;Cooling;
Stage #2: L-phenylalaninewith 4-methyl-morpholine in tetrahydrofuran;Inert atmosphere;Cooling;
References:
Zhao, Ming;Liu, Jiangyuan;Zhang, Xiaoyi;Peng, Li;Li, Chunyu;Peng, Shiqi [Bioorganic and Medicinal Chemistry,2009,vol. 17,# 10,p. 3680 - 3689] Location in patent:supporting information; experimental part
7647-01-0
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$10.00/10g
26048-69-1
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150-30-1
566 suppliers
$10.00/25G
68763-45-1
30 suppliers
$60.00/500mg
7536-58-5
329 suppliers
$6.00/5g
68763-45-1
30 suppliers
$60.00/500mg
![L-Aspartic acid, N-[(1,1-dimethylethoxy)carbonyl]-, 1-anhydride with 2-methylpropyl hydrogen carbonate, 4-(phenylmethyl) ester](/CAS/20211123/GIF/84890-97-1.gif)
84890-97-1
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68763-45-1
30 suppliers
$60.00/500mg
7536-58-5
329 suppliers
$6.00/5g
13734-34-4
556 suppliers
$5.50/5g
68763-45-1
30 suppliers
$60.00/500mg