BOC-LEU-CHLOROMETHYLKETONE synthesis

2synthesis methods

Product Name:BOC-LEU-CHLOROMETHYLKETONE
CAS Number:102123-85-3
Molecular formula:C12H22ClNO3
Molecular Weight:263.76

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102123-85-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) isopropenyl chloroformate, di-isopropylethylamine / 1.) ethyl acetate, -10 deg C, 5 min, 2.) diethyl ether, 0 deg C, 30 min
2: 87 percent / 3 M HCl / diethyl ether

References:

Dufour, Marie-Noelle;Jouin, Patrick;Poncet, Joel;Pantaloni, Antoine;Castro, Bertrand [Journal of the Chemical Society. Perkin transactions I,1986,p. 1895 - 1900]

N-alpha-t-Butyloxycarbonyl-L-leucinyl-diazomethane, (S)-3-Boc-amino-1-diazo-5-methyl-2-hexanone

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102123-85-3
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References