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ChemicalBook CAS DataBase List BRN 4488383
77529-42-1

BRN 4488383 synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 70percent HClO4, Tl(NO3)3 / Ambient temperature
2: 50 percent / NH3 / methanol / 96 h / Ambient temperature
3: 50 percent / t-BuOK / dimethylformamide / Ambient temperature

References:

Rooney;Randall;Streeter;Ziegler;Cragoe Jr.;Schwam;Michelson;Williams;Eichler;Duggan;Ulm;Noll [Journal of Medicinal Chemistry,1983,vol. 26,# 5,p. 700 - 714]