Carbamic acid cyclohexyl ester synthesis
- Product Name:Carbamic acid cyclohexyl ester
- CAS Number:1124-54-5
- Molecular formula:
- Molecular Weight:0
Yield:1124-54-5 94%
Reaction Conditions:
with pyridine at 0 - 20; for 0.5 h;Green chemistry;
Steps:
General procedure synthesis of primary carbamates
General procedure: Alcohol (1 mmol, 2a-g) was dissolved in 5mL pyridine. Thereaction mixture was cooled to 0 C and chlorosulfonyl isocyanate(CSI, 1.1 mmol) was added and resulting solutionwas stirred for 0.5 h at the room temperature. The reactionmixture was extracted with EtOAc. The organic phase wasdried over sodium sulfate and concentrated. Purification wasperformed through thin-layer chromatography (TLC) on silicagel.
References:
Atmaca, Ufuk;Aksoy, Mine;?ztekin, Aykut [Journal of Biomolecular Structure and Dynamics,2022]
13248-54-9
120 suppliers
inquiry
1124-54-5
4 suppliers
inquiry