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CHEMBRDG-BB 5874535 synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 88 percent / p-toluenesulfonic acid / toluene / 5 h / Heating
2: NaBH4 / ethanol / 1 h / 20 °C

References:

Akalaeva, T. V.;Bokanov, A. I.;Ivanov, P. Yu.;Nikolaeva, I. S.;Pushkina, T. V.;et al. [Pharmaceutical Chemistry Journal,1989,vol. 23,# 3,p. 231 - 234][Khimiko-Farmatsevticheskii Zhurnal,1989,vol. 23,# 3,p. 299 - 302]