ChemicalBook CAS DataBase List Chrysin 6-C-glucoside

Chrysin 6-C-glucoside synthesis

2synthesis methods

Product Name:Chrysin 6-C-glucoside
CAS Number:28368-57-2
Molecular formula:C21H20O9
Molecular Weight:416.38

1-(2,4-bis (benzyloxy)-6-hydroxyphenyl) ethanone

18065-05-9
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28368-57-2
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160880-89-7
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / Reflux
2: potassium hydroxide / pyridine / 1 h / 85 °C / Inert atmosphere
3: hydrogen; palladium 10% on activated carbon / methanol; tetrahydrofuran
4: recombinant Oryza sativa C-glycosyltransferase / ethanol / 30 °C / pH 7.5 / Enzymatic reaction

References:

Hao;Caulfield;Hamilton;Pickett;Midega;Khan;Wang;Hooper [Phytochemistry,2016,vol. 125,p. 73 - 87]

Ethanone, 1-[2-(benzoyloxy)-4,6-bis(phenylmethoxy)phenyl]-

137790-51-3
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28368-57-2
8 suppliers
inquiry

160880-89-7
4 suppliers
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References

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