CI 992 synthesis

2synthesis methods

Product Name:CI 992
CAS Number:135704-06-2
Molecular formula:C33H52N6O7S2
Molecular Weight:708.93

L-Alaninamide, N-(4-morpholinylsulfonyl)-L-phenylalanyl-N-[1-(cyclohexylmethyl)-2,3-dihydroxy-5-methylhexyl]-3-[2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-4-thiazolyl]-, [1S-(1R*,2S*,3R*)]- (9CI)

135704-12-0
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135704-06-2
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Yield:135704-06-2 84%

Reaction Conditions:

with ammonium chloride;zinc in tetrahydrofuran;methanol; for 9.5 h;Ambient temperature;

References:

Patt, William C.;Hamilton, Harriet W.;Taylor, Michael D.;Ryan, Michael J.;Taylor, David G.;et al. [Journal of Medicinal Chemistry,1992,vol. 35,# 14,p. 2562 - 2572]

4-Thiazolepropanoic acid, α-[[(1,1-dimethylethoxy)carbonyl]amino]-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-, phenylmethyl ester, (S)- (9CI)

135703-86-5
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135704-06-2
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References

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