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ChemicalBook CAS DataBase List cis--ethyl 3-(benzyloxy)cyclobutanecarboxylate
141352-62-7

cis--ethyl 3-(benzyloxy)cyclobutanecarboxylate synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
2: aq. 4M KOH / H2O; ethanol / 5 h / Heating
3: 88.6 percent / 215 °C / 0.4 Torr
4: 99.5 percent / oxalyl chloride / CCl4 / 1) 0 deg C, 1 h, 2) r.t., 12 h
5: CCl4 / 5 h / Ambient temperature

References:

Henlin;Rink;Spieser;Baschang [Helvetica Chimica Acta,1992,vol. 75,# 2,p. 589 - 603]