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13763-19-4

Cl10Si4 synthesis

2synthesis methods
-

Yield:13763-19-4 92%

Reaction Conditions:

with HCl;AlCl3 in benzene;to a suspn. of tetrasilane in benzene a small amount of AlCl3 was added, heated to 50°, HCl(g) was passed for 20 min; evapd., heptane was added, distilled (65°C, 0.05 mbar);

References:

Zink, Robert;Magnera, Thomas F.;Michl, Josef [Journal of Physical Chemistry A,2000,vol. 104,# 16,p. 3829 - 3841]