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40143-78-0

CPRNWMZKNOIIML-UHFFFAOYSA-N synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: ethylmagnesium bromide / diethyl ether / 1 h / -78 °C / Inert atmosphere
1.2: 6 h / -78 °C / Inert atmosphere
2.1: water / diethyl ether / 0 °C / Inert atmosphere
3.1: dihydrogen peroxide / diethyl ether / Inert atmosphere

References:

Hosein, Adil I.;Le Goff, Xavier F.;Ricard, Louis;Caffyn, Andrew J. M. [Inorganic Chemistry,2011,vol. 50,# 4,p. 1484 - 1490]