Cyclohexanamine, 2-phenyl- synthesis
- Product Name:Cyclohexanamine, 2-phenyl-
- CAS Number:17293-45-7
- Molecular formula:C12H17N
- Molecular Weight:175.27
1444-65-1
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Yield:17293-45-7 62%
Reaction Conditions:
Stage #1: (RS)-2-phenylcyclohexanonewith titanium(IV) isopropylate;ammonium chloride;triethylamine in ethanol at 20; for 11 h;Addition;
Stage #2: with sodium tetrahydroborate in ethanol at 20; for 8 h;Reduction;
References:
Bhattacharyya, Sukanta;Neidigh, Kurt A.;Avery, Mitchell A.;Williamson, John S. [Synlett,1999,# 11,p. 1781 - 1783]
771-98-2
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5758-09-8
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17293-45-7
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