Cyclohexanol,1-(bromomethyl)- synthesis
- Product Name:Cyclohexanol,1-(bromomethyl)-
- CAS Number:17299-10-4
- Molecular formula:C7H13BrO
- Molecular Weight:193.08
Yield:17299-10-4 86%
Reaction Conditions:
Stage #1: 1,1-dibromomethanewith titanium tetrachloride;magnesium at 0; for 0.0166667 h;Inert atmosphere;
Stage #2: cyclohexanone in 1,2-dimethoxyethane;1,2-dichloro-ethane at 0; for 3 h;Inert atmosphere;
References:
Yan, Tu Hsin;Ananthan, Bakthavachalam;Chang, Su Haur [European Journal of Organic Chemistry,2019,vol. 2019,# 4,p. 778 - 787]
1192-37-6
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17299-10-4
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