(cyclohexylmethyl) triphenylphosphonium iodide synthesis
1synthesis methods
- Product Name:(cyclohexylmethyl) triphenylphosphonium iodide
- CAS Number:91312-70-8
- Molecular formula:C25H28IP
- Molecular Weight:486.38
![Benzene, [(1E)-4-cyclohexyl-1,3-butadien-1-yl]-](/CAS/20210305/GIF/682344-63-4.gif)
Yield:682344-63-4 97%
Reaction Conditions:
Stage #1: (cyclohexylmethyl)triphenylphosphonium iodidewith potassium tert-butylate in tetrahydrofuran; for 15 h;
Stage #2: (E)-3-phenylpropenal in tetrahydrofuran;
References:
Taylor, Dennis K.;Avery, Thomas D.;Greatrex, Ben W.;Tiekink, Edward R. T.;Macreadie, Ian G.;Macreadie, Peter I.;Humphries, Adam D.;Kalkanidis, Martha;Fox, Emma N.;Klonis, Nectarios;Tilley, Leann [Journal of Medicinal Chemistry,2004,vol. 47,# 7,p. 1833 - 1839]