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ChemicalBook CAS DataBase List CYCLOPENTA(C,D)PYRENE
27208-37-3

CYCLOPENTA(C,D)PYRENE synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 70 percent / polyphosphoric acid / 2 h / 70 - 125 °C
2: sodium borohydride / tetrahydrofuran / 2 h / Ambient temperature
3: 83 percent / paratoluenesulfonic acid / toluene / 1 h / Heating

References:

Tintel, C.;Cornelisse, J.;Lugtenburg, J. [Recueil des Travaux Chimiques des Pays-Bas,1983,vol. 102,# 1,p. 14 - 20]