Cyclopentanemethylamine synthesis
- Product Name:Cyclopentanemethylamine
- CAS Number:6053-81-2
- Molecular formula:C6H13N
- Molecular Weight:99.17
4254-02-8
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6053-81-2
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Yield: 84%
Reaction Conditions:
with sodium sulfate
Steps:
13.a 2-[5-(N-Cyclopentylmethylcarbamoyl)-3-[2-methoxy-4-[2-(phenylsulphonyl)acetyl]benzyl]indol-1-yl]-N,N-dimethylpropionamide
(a) A solution of cyclopentylnitrile (15 g) in ether (115 ml) was added dropwise, under nitrogen, to a refluxing slurry of lithium aluminum hydride (9 g) in ether (200 ml). The mixture was treated with a saturated aqueous solution of sodium sulfate and filtered. The filtrate was dried (MgSO4) and evaporated to give cyclopentylmethylamine (13 g, 84%) as a yellow liquid; IR (neat): 3300, 3340, 1600 cm-1.
References:
ICI Americas Inc. US4837235, 1989, A
70341-45-6
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6053-81-2
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1123-00-8
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6053-81-2
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