Cyclopentene,1-propyl- synthesis
- Product Name:Cyclopentene,1-propyl-
- CAS Number:3074-61-1
- Molecular formula:C8H14
- Molecular Weight:110.2
120-92-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 70 percent / tetrahydrofuran / 0.5 h / Ambient temperature
2: 1.) n-BuLi, TMEDA / 1.) hexane, -78 deg C, 15 min, 2.) a) -78 deg C, 30 min, b) 0 deg C, 15 min, c) RT, 30 min
3: 62 percent / Ph3P, CCl4 / 15 h / Heating
4: Li, 1percent Na / tetrahydrofuran / 2 h / Irradiation
References:
Engel, Paul S.;Culotta, Anne Marie [Journal of the American Chemical Society,1991,vol. 113,# 7,p. 2686 - 2696]
132439-45-3
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3074-61-1
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64027-99-2
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1604-02-0
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3524-75-2
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