DC0-NH2 synthesis
- Product Name:DC0-NH2
- CAS Number:615538-51-7
- Molecular formula:C31H24ClN5O3
- Molecular Weight:550.01
16732-57-3
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Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 2068.65 Torr
2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / Inert atmosphere
3.1: sodium hydroxide / N,N-dimethyl acetamide; water / 1 h
3.2: pH 3
4.1: N,N-dimethyl acetamide; 1,2-dichloro-ethane / Inert atmosphere
5.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / N,N-dimethyl acetamide
References:
Zhao, Robert Yongxin;Erickson, Hans K.;Leece, Barbara A.;Reid, Emily E.;Goldmacher, Victor S.;Lambert, John M.;Chari, Ravi V. J. [Journal of Medicinal Chemistry,2012,vol. 55,# 2,p. 766 - 782]
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