DDMS synthesis
- Product Name:DDMS
- CAS Number:2642-80-0
- Molecular formula:C14H11Cl3
- Molecular Weight:285.6
Yield:2642-80-0 86%
Reaction Conditions:
Stage #1: Chloroiodomethane;4,4'-Dichlorobenzophenonewith methyllithium lithium bromide in tetrahydrofuran at -78; for 0.75 h;Inert atmosphere;
Stage #2: with hexylsilane;tris(pentafluorophenyl)borate in dichloromethane at 20; for 1 h;Inert atmosphere;chemoselective reaction;
References:
Citarella, Andrea;Holzer, Wolfgang;Ielo, Laura;Langer, Thierry;Miele, Margherita;Pace, Vittorio;Urban, Ernst;Zehl, Martin [Organic Letters,2020,vol. 22,# 19,p. 7629 - 7634] Location in patent:supporting information
72-54-8
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$32.00/100mg
1022-22-6
40 suppliers
$115.00/250mg
2642-80-0
8 suppliers
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20851-90-5
2 suppliers
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50-29-3
106 suppliers
$28.00/1mg
1022-22-6
40 suppliers
$115.00/250mg
72-55-9
133 suppliers
$28.00/50mg
![1-chloro-4-[1-(4-chlorophenyl)ethyl]benzene](/CAS/GIF/3547-04-4.gif)
3547-04-4
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2642-80-0
8 suppliers
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50-29-3
106 suppliers
$28.00/1mg
2642-80-0
8 suppliers
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72-54-8
139 suppliers
$32.00/100mg
2642-80-0
8 suppliers
inquiry