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ChemicalBook CAS DataBase List DI-N-BUTYLTELLURIUM
38788-38-4

DI-N-BUTYLTELLURIUM synthesis

9synthesis methods
Dibutyl telluride and diisobutyl telluride are prepared from n-butyl bromide and  isobutyl bromide with Sodium Telluride, which is prepared in situ from Tellurium powder, rongalite  (Sodium Hydroxymethanesulfinate), and Sodium Hydroxide in H2O.
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Yield:38788-38-4 97%

Reaction Conditions:

with triphenyl phosphite;potassium carbonate in toluene at 80;

References:

Huang, Zheng-Zheng;Tang, Yong [Journal of Organic Chemistry,2002,vol. 67,# 15,p. 5320 - 5326]

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