DI-t-BUTYLISOBUTYLSILANE synthesis
- Product Name:DI-t-BUTYLISOBUTYLSILANE
- CAS Number:1314639-85-4
- Molecular formula:C12H28Si
- Molecular Weight:200.44
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Yield:-
Reaction Conditions:
Stage #1:isobutyltrichlorosilane;tert.-butyl lithium in n-heptane for 15 h;Inert atmosphere;Reflux;
Stage #2: with isopropyl alcohol in n-heptane at 0;Inert atmosphere;
References:
Liang, Huan;Hu, Lin;Corey [Organic Letters,2011,vol. 13,# 15,p. 4120 - 4123] Location in patent:supporting information; experimental part