DIALLYLCARBAMYL CHLORIDE synthesis
- Product Name:DIALLYLCARBAMYL CHLORIDE
- CAS Number:25761-72-2
- Molecular formula:C7H10ClNO
- Molecular Weight:159.61
124-02-7
254 suppliers
$14.00/5mL
25761-72-2
54 suppliers
$18.00/100mg
Yield:-
Reaction Conditions:
in ethyl acetate
Steps:
2 EXAMPLE 2
To the refluxing, stirred solution was added dropwise a solution of diallylamine (50 g.) in ethyl acetate (100 ml.), maintaining a brisk flow of phosgene. The rate of addition of the solution of diallylamine was such that solid diallylamine hydrochloride did not accumulate in the reaction mixture. When the addition was complete, the flow of phosgene into the stirred, refluxing reaction mixture was maintained for 30 minutes. The reaction mixture was distilled under reduced pressure to remove the solvent and give the product, diallylcarbamoyl chloride, as an oil, b.p. 67° - 69°C./3 mm.
References:
The Boots Company Limited US3952001, 1976, A
32315-10-9
441 suppliers
$10.00/1g
124-02-7
254 suppliers
$14.00/5mL
25761-72-2
54 suppliers
$18.00/100mg
124-02-7
254 suppliers
$14.00/5mL
503-38-8
124 suppliers
$15.00/5g
25761-72-2
54 suppliers
$18.00/100mg
