Dicyclohexylborane synthesis
- Product Name:Dicyclohexylborane
- CAS Number:1568-65-6
- Molecular formula:C12H23B
- Molecular Weight:178.12
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Yield:-
Reaction Conditions:
in tetrahydrofuran at 0; for 1 h;
Steps:
1.1.1
A 250 mL flask equipped with a septum inlet and magnetic stir bar was charged with 50 mmol of BH3SMe2 and 18 mL of freshly distilled THF. It was cooled to 0° C. and 115 mmol of cyclohexene was added dropwise. After the mixture was stirred at 0° C. for 1 hour, (C6H11)2BH separates as a white solid.
References:
Amyris Biotechnologies US2006/270863, 2006, A1 Location in patent:Page/Page column 17
110-83-8
319 suppliers
$11.00/25g
1568-65-6
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13292-87-0
249 suppliers
$18.19/5ml
1568-65-6
31 suppliers
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![Boron, dihydro[1,1'-thiobis[methane]]-](/CAS/20210111/GIF/111532-78-6.gif)
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110-83-8
319 suppliers
$11.00/25g
1568-65-6
31 suppliers
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