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ChemicalBook CAS DataBase List Dihydropinosylvin

Dihydropinosylvin synthesis

13synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) n-butyl Li / 1.) THF, hexane, 30 min; 2.) 0 deg C, THF, 30 min
2: 100 percent / hydrogen / 5percent Pd-C / ethanol / 1 h / Ambient temperature
3: 90 percent / BBr3 / CH2Cl2 / 1.) -70 deg C; 2.) room temperature, 1.5 h

References:

Mitscher, Lester A.;Park, Young Han;Al-Shamma, Ali;Hudson, P. Bryan;Haas, Thomas [Phytochemistry,1981,vol. 20,# 4,p. 781 - 786]

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