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ChemicalBook CAS DataBase List DIPYRIDIN-3-YLMETHANONE
35779-35-2

DIPYRIDIN-3-YLMETHANONE synthesis

13synthesis methods
-

Yield:35779-35-2 76%

Reaction Conditions:

Stage #1: 3-Bromopyridine;n-butyllithium in diethyl ether;hexane at -78; for 0.5 h;
Stage #2: methyl 3-pyridinecarboxylate in diethyl ether;benzene at -78 - -20;

References:

Chen, Xu-Dong;Mak, Thomas C.W. [Journal of Molecular Structure,2005,vol. 743,# 1-3,p. 1 - 6]