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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Dizocilpine

Dizocilpine synthesis

3synthesis methods
5H-Dibenzo[a,d]cyclohepten-5,10-imine-5-methanol, 10,11-dihydro-, (5S,10R)-

380427-51-0
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Dizocilpine

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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: HCO2Et
1.2: 81 percent / SOBr2; aq. HBr
2.1: 85 percent / LiBHEt3 / tetrahydrofuran / 3 h / 60 °C

References:

Funabashi;Ratni;Kanai;Shibasaki [Journal of the American Chemical Society,2001,vol. 123,# 43,p. 10784 - 10785]

5H-Dibenzo[a,d]cyclohepten-5,10-imine, 5-(bromomethyl)-10,11-dihydro-, (5S,10R)-

159170-13-5
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Dizocilpine

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References
5H-Dibenzo[a,d]cyclohepten-5,10-imine-12-carboxylic acid, 5-cyano-10,11-dihydro-, ethenyl ester, (5S,10R)-

380427-50-9
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Dizocilpine

77086-21-6
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References

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