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ChemicalBook CAS DataBase List (E)-9-Octadecene
7206-25-9

(E)-9-Octadecene synthesis

14synthesis methods
-

Yield: 24.39 %Chromat. , 16.2 %Chromat. , 8.29 %Chromat.

Reaction Conditions:

in hexane at 45; for 5 h;Inert atmosphere;

Steps:

Metathesis reaction
General procedure: Metathesis reactions were carried out in small quartz batch reactor containing inert atmosphere. Typically, methyloleate (50 μL) in 500 μL hexane was added to the catalyst (50 mg) in dry conditions at the investigated temperature (45 °C) with stirring at 400 rpm for 5 h. The reaction was then stopped by addition of acetone enabling desorption of the reactants and products from the catalytic surface

References:

Pillai, Subha Kumaraswamy;Hamoudi, Safia;Belkacemi, Khaled [Applied Catalysis A: General,2013,vol. 455,p. 155 - 163]