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ChemicalBook CAS DataBase List (-)-ECG-3''-O-ME

(-)-ECG-3''-O-ME synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: oxalyl chloride; DMF / CH2Cl2 / 3 h / Heating
2: 300 mg / DMAP / CH2Cl2 / 20 °C
3: 80 percent / H2 / Pd(OH)2/C / tetrahydrofuran; methanol / 6 h / 20 °C

References:

Wan, Sheng Biao;Ping Dou;Chan, Tak Hang [Tetrahedron,2006,vol. 62,# 25,p. 5897 - 5904]

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