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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List (-)-epibatidine-l-tartrate
152378-30-8

(-)-epibatidine-l-tartrate synthesis

5synthesis methods
69045-79-0 Synthesis
2-Chloro-5-iodopyridine

69045-79-0
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(-)-epibatidine-l-tartrate

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-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: n-BuLi / diethyl ether; tetrahydrofuran; hexane / 1.) -70 deg C, 20 min, 2.) -70 deg C, 2 h; -50 deg C, 30 min
2: KH / tetrahydrofuran / 1.) r.t., 20 min, 2.) r.t., 20 min
3: toluene / 2 h / Heating
4: H2 / PtO2 / ethyl acetate / 1 h / 2068.6 Torr
5: HCl / ethyl acetate / 1 h / 0 °C

References:

Fletcher, Stephen R.;Baker, Raymond;Chambers, Mark S.;Herbert, Richard H.;Hobbs, Sarah C.;et al. [Journal of Organic Chemistry,1994,vol. 59,# 7,p. 1771 - 1778]

N-(CYCLOHEX-3-ENYL)-2,2,2-TRIFLUOROACETAMIDE

78293-47-7
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(-)-epibatidine-l-tartrate

152378-30-8
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References
Acetamide, N-3-cyclohexen-1-yl-2,2,2-trifluoro-N-(phenylmethyl)-

152533-42-1
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(-)-epibatidine-l-tartrate

152378-30-8
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References
7-Azabicyclo[2.2.1]heptane-7-carboxylic acid, 2-hydroxy-, 1,1-dimethylethyl ester, (1S-exo)- (9CI)

154905-38-1
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(-)-epibatidine-l-tartrate

152378-30-8
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References
tert-butyl (1S,4R)-2-oxo-7-azabicyclo[2.2.1]heptane-7-carboxylate

163513-99-3
24 suppliers
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(-)-epibatidine-l-tartrate

152378-30-8
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References

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