ChemicalBook CAS DataBase List erycibelline

erycibelline synthesis

2synthesis methods

Product Name:erycibelline
CAS Number:107633-95-4
Molecular formula:C7H13NO2
Molecular Weight:143.18

2H-Pyrrole-2-propanal, 3,4-dihydro-4-(phenylmethoxy)-, 1-oxide, (2R,4R)-

1345989-13-0
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107633-95-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: samarium diiodide; tert-butyl alcohol / tetrahydrofuran / -78 °C / Inert atmosphere
2: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water / 2 h / 20 °C
3: copper diacetate; iron; acetic acid / 20 °C

References:

Zhang, Zhao-Lan;Nakagawa, Shinpei;Kato, Atsushi;Jia, Yue-Mei;Hu, Xiang-Guo;Yu, Chu-Yi [Organic and Biomolecular Chemistry,2011,vol. 9,# 22,p. 7713 - 7719]

8-Azabicyclo[3.2.1]octane-2,7-diol, 8-hydroxy-, (1S,2S,5R,7R)-

1345989-15-2
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107633-95-4
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References