Ethane, 1,2-bis(2-bromoethoxy)- synthesis
- Product Name:Ethane, 1,2-bis(2-bromoethoxy)-
- CAS Number:31255-10-4
- Molecular formula:C6H12Br2O2
- Molecular Weight:275.97
112-27-6
772 suppliers
$6.00/100g
31255-10-4
86 suppliers
$183.30/0.5g
Yield: 90%
Reaction Conditions:
Stage #1:2,2'-[1,2-ethanediylbis(oxy)]bisethanol with carbon tetrabromide in dichloromethane for 0.25 h;Appel reaction;
Stage #2: with triphenylphosphine in dichloromethane at 20;Appel reaction;
References:
Hurley, Christopher A.;Wong, John B.;Ho, Jimmy;Writer, Michele;Irvine, Scott A.;Lawrence, M. Jayne;Hart, Stephen L.;Tabor, Alethea B.;Hailes, Helen C. [Organic and Biomolecular Chemistry,2008,vol. 6,# 14,p. 2554 - 2559] Location in patent:supporting information; experimental part
80322-82-3
31 suppliers
$80.00/500mg
31255-10-4
86 suppliers
$183.30/0.5g
507-16-4
72 suppliers
$15.00/5g
112-27-6
772 suppliers
$6.00/100g
31255-10-4
86 suppliers
$183.30/0.5g
19249-03-7
231 suppliers
$9.00/1g
31255-10-4
86 suppliers
$183.30/0.5g
1462-35-7
16 suppliers
inquiry
31255-10-4
86 suppliers
$183.30/0.5g