Ethanone, 1-(3-hydroxy-2-methylphenyl)- (9CI) synthesis

3synthesis methods

Product Name:Ethanone, 1-(3-hydroxy-2-methylphenyl)- (9CI)
CAS Number:69976-81-4
Molecular formula:C9H10O2
Molecular Weight:150.17

Preparation by diazotization of 6-amino-3-hydroxy-2- methylacetophenone, followed by hydrolysis of the obtained diazonium salt in the presence of hypophosphorous acid at 0° (42%).

24487-92-1
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Ethanone, 1-(3-hydroxy-2-methylphenyl)- (9CI)

69976-81-4
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Yield:69976-81-4 86%

Reaction Conditions:

with aluminum (III) chloride in chlorobenzene; for 5 h;Reflux;

References:

Qian, Yong;Schürmann, Marc;Janning, Petra;Hedberg, Christian;Waldmann, Herbert [Angewandte Chemie - International Edition,2016,vol. 55,# 27,p. 7766 - 7771][Angew. Chem.,2016,vol. 128,p. 7897 - 7902] Location in patent:supporting information

603-80-5
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$14.00/1g

917-54-4
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$52.10/25ml

69976-81-4
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References

55289-06-0
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$21.00/5g

69976-81-4
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References