ethyl 2-(5-methylthiophen-3-yl)acetate synthesis

1synthesis methods

Product Name:ethyl 2-(5-methylthiophen-3-yl)acetate
CAS Number:1261844-84-1
Molecular formula:C9H12O2S
Molecular Weight:184.26

Propanedioic acid, 2-(5-methyl-3-thienyl)-, 1,3-diethyl ester

1312573-91-3
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1261844-84-1
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Yield:1261844-84-1 80%

Reaction Conditions:

with sodium chloride in water;dimethyl sulfoxide at 155; for 8 h;

References:

Schnapperelle, Ingo;Breitenlechner, Stefan;Bach, Thorsten [Organic Letters,2011,vol. 13,# 14,p. 3640 - 3643] Location in patent:supporting information; experimental part

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