ethyl 2-chloro-6-fluoro-benzoat synthesis
- Product Name:ethyl 2-chloro-6-fluoro-benzoat
- CAS Number:773134-56-8
- Molecular formula:C9H8ClFO2
- Molecular Weight:202.61
443-26-5
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$14.00/5g
773134-56-8
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$132.00/1g
Yield:773134-56-8 52%
Reaction Conditions:
with sodium persulfate;N-chloro-succinimide;trifluorormethanesulfonic acid;palladium diacetate in 1,2-dichloro-ethane at 90; for 1.5 h;Sealed tube;regioselective reaction;
References:
Sun, Xiuyun;Shan, Gang;Sun, Yonghui;Rao, Yu [Angewandte Chemie - International Edition,2013,vol. 52,# 16,p. 4440 - 4444][Angew. Chem.,2013,vol. 125,# 16,p. 4536 - 4540,5] Location in patent:supporting information