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ChemicalBook CAS DataBase List ethyl 3-iodo-5-methoxybenzoate
717109-27-8

ethyl 3-iodo-5-methoxybenzoate synthesis

2synthesis methods
74165-74-5 Synthesis
3-Amino-5-methoxybenzoic acid

74165-74-5
75 suppliers
$41.39/1g

ethyl 3-iodo-5-methoxybenzoate

717109-27-8
33 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: thionyl chloride / 80 °C / Cooling with ice; Inert atmosphere
2.1: sodium nitrite; sulfuric acid / water / 0.5 h / -5 °C
2.2: 20 °C

References:

Granchi, Carlotta;Lapillo, Margherita;Glasmacher, Sandra;Bononi, Giulia;Licari, Cristina;Poli, Giulio;El Boustani, Maguie;Caligiuri, Isabella;Rizzolio, Flavio;Gertsch, Jürg;Macchia, Marco;Minutolo, Filippo;Tuccinardi, Tiziano;Chicca, Andrea [Journal of Medicinal Chemistry,2019,vol. 62,# 4,p. 1932 - 1958]

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