Ethyl fluoroacetate synthesis

12synthesis methods

Product Name:Ethyl fluoroacetate
CAS Number:4792-10-3
Molecular formula:C21H26N2O6
Molecular Weight:402.44

1H-Pyrrole-3-propanoic acid, 2,2'-methylenebis[5-carboxy-4-methyl-, α,α'-dimethyl ester

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Yield:4792-10-3 87%

Reaction Conditions:

Stage #1: 4,4'-bis-(2-methoxycarbonyl-ethyl)-3,3'-dimethyl-5,5'-methanediyl-bis-pyrrole-2-carboxylic acidwith trifluoroacetic acid at 0; for 1.16667 h;Inert atmosphere;
Stage #2: with trimethyl orthoformate at 0 - 5;Inert atmosphere;

References:

Martin, Pierre;Mueller, Markus;Flubacher, Dietmar;Boudier, Andreas;Blaser, Hans-Ulrich;Spielvogel, Dirk [Organic Process Research and Development,2010,vol. 14,# 4,p. 799 - 804] Location in patent:experimental part

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149-73-5 Synthesis