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ChemicalBook CAS DataBase List Ethyl fluoroacetate
4792-10-3

Ethyl fluoroacetate synthesis

12synthesis methods
-

Yield:4792-10-3 87%

Reaction Conditions:

Stage #1: 4,4'-bis-(2-methoxycarbonyl-ethyl)-3,3'-dimethyl-5,5'-methanediyl-bis-pyrrole-2-carboxylic acidwith trifluoroacetic acid at 0; for 1.16667 h;Inert atmosphere;
Stage #2: with trimethyl orthoformate at 0 - 5;Inert atmosphere;

References:

Martin, Pierre;Mueller, Markus;Flubacher, Dietmar;Boudier, Andreas;Blaser, Hans-Ulrich;Spielvogel, Dirk [Organic Process Research and Development,2010,vol. 14,# 4,p. 799 - 804] Location in patent:experimental part