Ethyl (R)-Piperidine-2-Carboxylate synthesis

1synthesis methods

Product Name:Ethyl (R)-Piperidine-2-Carboxylate
CAS Number:22328-77-4
Molecular formula:C8H15NO2
Molecular Weight:157.21

2-Pyridinecarboxylic acid, 1,2,3,4-tetrahydro-1-(4-methoxyphenyl)-4-oxo-, ethyl ester

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: H₂ / 20 percent PtO₂ / ethyl acetate / 80 h / 20 °C
2: toluene / 6 h / 110 °C
3: 99 percent / Bu₃SnH; AIBN / toluene / 4 h / 90 °C
4: (NH₄)2Ce(NO₃)6; H₂O / acetonitrile / 0.33 h / 0 °C

References:

Yao, Sulan;Saaby, Steen;Hazell, Rita G.;Jorgensen, Karl Anker [Chemistry - A European Journal,2000,vol. 6,# 13,p. 2435 - 2448]

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