Ethyl5-bromo-3-hydroxy-1H-indole-2-carboxylate synthesis
- Product Name:Ethyl5-bromo-3-hydroxy-1H-indole-2-carboxylate
- CAS Number:153501-30-5
- Molecular formula:C11H10BrNO3
- Molecular Weight:284.11
100123-25-9
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153501-30-5
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$596.00/1g
Yield:153501-30-5 86%
Reaction Conditions:
Stage #1: ethyl 5-bromo-3-formyl-1H-indole-2-carboxylatewith toluene-4-sulfonic acid;3-chloro-benzenecarboperoxoic acid in dichloromethane at 10;Baeyer-Villiger oxidation;
Stage #2: with dimethylsulfide;ethanol
References:
Hickman;Sturino;Lachance [Tetrahedron Letters,2000,vol. 41,# 43,p. 8217 - 8220]
![Benzoic acid, 5-bromo-2-[(2-ethoxy-2-oxoethyl)amino]-, ethyl ester](/CAS/20210305/GIF/153501-29-2.gif)
153501-29-2
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153501-30-5
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$596.00/1g
63243-76-5
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$60.00/50mg
153501-30-5
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16732-70-0
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$6.00/1g
153501-30-5
33 suppliers
$596.00/1g