FMOC-3-(3'-QUINOLYL)-L-ALANINE synthesis
- Product Name:FMOC-3-(3'-QUINOLYL)-L-ALANINE
- CAS Number:281655-61-6
- Molecular formula:C27H22N2O4
- Molecular Weight:438.47
13669-42-6
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
1.2: 3 h / 20 °C / Inert atmosphere
2.1: (-)-1,2-bis-((2R,5R)-2,5-diethylphospholano)benzene(cyclooctadiene) rhodium(I) trifluoromethanesulfonate; hydrogen / ethyl acetate / 24 h / 50 °C / 30003 Torr / Inert atmosphere
3.1: hydrogenchloride / water / 6 h / 100 °C / Inert atmosphere
4.1: sodium carbonate / 1,4-dioxane / 48 h / 0 - 20 °C / Inert atmosphere
References:
Ramon, Rosario;Martin-Gago, Pablo;Verdaguer, Xavier;Macias, Maria J.;Martin-Malpartida, Pau;Fernandez-Carneado, Jimena;Gomez-Caminals, Marc;Ponsati, Berta;Lopez-Ruiz, Pilar;Cortes, Maria Alicia;Colas, Begona;Riera, Antoni [ChemBioChem,2011,vol. 12,# 4,p. 625 - 632]
1282534-49-9
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281655-61-6
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