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ChemicalBook CAS DataBase List FMOC-D-PHENYLALANYL CHLORIDE

FMOC-D-PHENYLALANYL CHLORIDE synthesis

1synthesis methods
86123-10-6 Synthesis
Fmoc-D-phenylalanine

86123-10-6
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FMOC-D-PHENYLALANYL CHLORIDE

103321-58-0
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Yield:103321-58-0 92.5%

Reaction Conditions:

with thionyl chloride;N,N-dimethyl-formamide in dichloromethane; for 1 h;Ambient temperature;

References:

Carpino, Louis A.;Cohen, Beri J.;Stephens, Kenton E.;Sadat-Aalaee, S. Yahya;Tien, Jien-Heh;Langridge, Denton C. [Journal of Organic Chemistry,1986,vol. 51,# 19,p. 3732 - 3734]

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