ChemicalBook CAS DataBase List galanolactone

galanolactone synthesis

3synthesis methods

Product Name:galanolactone
CAS Number:115753-79-2
Molecular formula:C20H30O3
Molecular Weight:318.45

515-03-7 Synthesis

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 65 percent / OsO₄, NaIO₄ / 2-methyl-propan-2-ol; tetrahydrofuran / 5.5 h / 25 °C
2: NaH / toluene / 1.) 0 deg C, 4 h, 2.) 80 deg C, 1 h
3: 71 percent / quinoline / 2 h / Heating
4: mCPBA / CHCl₃ / 0 °C

References:

Jung, Mankil;Lee, Seokjoon;Yoon, Byunghee [Tetrahedron Letters,1997,vol. 38,# 16,p. 2871 - 2874]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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115753-79-2
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References

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115753-79-2
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References

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