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ChemicalBook CAS DataBase List H-D-Glu-OBzl

H-D-Glu-OBzl synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
2: 1 h
3: sodium carbonate / 1,4-dioxane; water / 10 - 20 °C

References:

Agnihotri, Geetanjali;Ukani, Rehman;Malladi, Subbalakshmi S.;Warshakoon, Hemamali J.;Balakrishna, Rajalakshmi;Wang, Xinkun;David, Sunil A. [Journal of Medicinal Chemistry,2011,vol. 54,# 5,p. 1490 - 1510]

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