H-Val-CMK·HCl synthesis

1synthesis methods

Product Name:H-Val-CMK·HCl
CAS Number:107831-79-8
Molecular formula:C6H12ClNO.ClH
Molecular Weight:186.081

(3S)-3-BOC-AMINO-1-DIAZO-4-METHYL-2-PENTANONE

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107831-79-8
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Yield:107831-79-8 5.27 g

Reaction Conditions:

with hydrogenchloride in 1,4-dioxane;water at 0; for 2 h;

References:

Hauske, Patrick;Meltzer, Michael;Ottmann, Christian;Krojer, Tobias;Clausen, Tim;Ehrmann, Michael;Kaiser, Markus [Bioorganic and Medicinal Chemistry,2009,vol. 17,# 7,p. 2920 - 2924] Location in patent:experimental part

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