ChemicalBook CAS DataBase List Hercynine

Hercynine synthesis

2synthesis methods

Yield: 36%

Reaction Conditions:

Stage #1:N,N-dimethyl-L-histidine hydrochloride with ammonia in methanol;water; pH=9
Stage #2:methyl iodide in methanol;water at 20;

References:

Song, Heng;Leninger, Maureen;Lee, Norman;Liu, Pinghua [Organic Letters,2013,vol. 15,# 18,p. 4854 - 4857] Location in patent:supporting information

71-00-1 Synthesis

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