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ChemicalBook CAS DataBase List HNE
75899-68-2

HNE synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 83 percent / tetrahydrofuran / 0.25 h / 0 °C
2: 64 percent / TBAF / tetrahydrofuran; dimethylformamide / 5 h / 20 °C
3: 42 percent / 5 h / Irradiation
4: methanol / Irradiation

References:

Brinson, Robert G.;Jones, Paul B. [Organic Letters,2004,vol. 6,# 21,p. 3767 - 3770]

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