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ChemicalBook CAS DataBase List inositol 3-phosphate

inositol 3-phosphate synthesis

4synthesis methods
114828-08-9 Synthesis
(1R,2S,3r,4R,5S,6s)-2,4,6-tris(benzyloxy)cyclohexane-1,3,5-triol

114828-08-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 56 percent / Boc-π(Me)-t-BuHyp-spiro-5-Tyr(O-t-Bu)-Phe-OMe; Et3N / toluene; CH2Cl2 / 4 h / 0 °C
2: 95 percent / Li; NH3(liq.) / tetrahydrofuran

References:

Sculimbrene, Bianca R.;Morgan, Adam J.;Miller, Scott J. [Journal of the American Chemical Society,2002,vol. 124,# 39,p. 11653 - 11656]