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Isophosphinoline synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: (i) SOCl2, CHCl3, (ii) LiAlH4, THF, Et2O
2: (i) COCl2, toluene, (ii) Et3N

References:

de Graaf,H.G.;Bickelhaupt,F. [Tetrahedron,1975,vol. 31,p. 1097 - 1103]